Polyether_Polyether Polyol Knowledge triphenylmethane chloride

triphenylmethane chloride

Triphenylmethane Structural Formula

Structural formula

Business number 04AP
Molecular formula C19H15BF4
Molecular weight 330.13
label

Trityltetrafluoroborate,

triphenyltetrafluoroborate carbon,

triphenyl-methyliutetrafluoroborate(1-),

Tritylium tetrafluoroborate,

Trityl fluoroborate,

Triphenylcarbenium tetrafluoroborate,

Triphenylmethyl tetrafluoroborate,

Trityl tetrafluoroborate,

Triphenylcarbeniumtetrafluoroborate,98%,

Methylium, triphenyl-, tetraflu

Numbering system

CAS number:341-02-6

MDL number:MFCD00013120

EINECS number:206-433-3

RTECS number:None

BRN number:5085649

PubChem number:24850086

Physical property data

1. Physical property data

Character: yellow solid

Density (g/mL, 25/4℃ ): Not available

Relative vapor density (g/mL, air=1): Not available

Melting point (ºC): 205- 215

Boiling point (ºC, normal pressure): Not available

Boiling point (ºC, 5.2kPa): Not available

Refractive index: Not available

Flash point (ºC): Not available

Specific rotation (º) : Not available

Autoignition point or ignition temperature (ºC): Not available

Vapor pressure (kPa, 25ºC): Not available

Saturated vapor pressure (kPa, 60ºC): Not available

Heat of combustion (KJ/mol): Not available

Critical temperature (ºC): Not available

Critical pressure (KPa): Not available

Oil and water (octanol /water) logarithmic value of the distribution coefficient: not available

Explosion upper limit (%, V/V): not available

Lower explosion limit ( %, V/V): Not available

Solubility: Not available

Toxicological data

2. Toxicological data:

Acute toxicity: Not available.

Ecological data

3. Ecological data:

1. Other harmful effects: This substance may be harmful to the environment, and special attention should be paid to water bodies.

Molecular structure data

None yet

Compute chemical data

1. Reference value for hydrophobic parameter calculation (XlogP): None

2. Number of hydrogen bond donors: 0

3. Number of hydrogen bond acceptors: 5

4. Number of rotatable chemical bonds: 3

5. Number of tautomers: none

6. Topological molecule polar surface area 0

7. Number of heavy atoms: 24

8. Surface charge: 0

9. Complexity: 215

10. Number of isotope atoms: 0

11. Determine the number of atomic stereocenters: 0

12. Uncertain number of atomic stereocenters: 0

13. Determine the number of chemical bond stereocenters: 0

14. Number of uncertain chemical bond stereocenters: 0

15. Number of covalent bond units: 2

Properties and stability

None yet

Storage method

Store at 2-8℃.

Synthesis method

1. In a 250 ml Erlenmeyer flask equipped with a magnetic stirrer and a nitrogen introduction tube, place 27.9 g (0.1 mol) of triphenyl chloride and 100 ml Thousand dry benzene. The mixture was stirred under dry nitrogen until a clear solution formed. Cool the solution to 0°C in an ice-salt bath. Add 13.4 grams (0.1 mol) of anhydrous monodimethyl ether tetrafluoroborate complex through the dropping funnel within 10 minutes, and continue stirring for 1 minute without further cooling. 50 ml of petroleum ether was added to the reaction mixture, and filtered through a glass core funnel. The bright yellow solid was washed with two 50 ml portions of petroleum ether, dried under a stream of dry nitrogen and then in vacuo. Get 2 grams (73%, melting point is about 200°C (decomposition).

Purpose

1. Same as trityl perchlorate, but more stable, so it is used more often. Alcohol oxidizing agent. Synthesis of alkenes.

Resource:allhdi.com

This article is from the Internet, does not represent the position of Toluene diisocyanate reproduced please specify the source.https://www.polyether-factory.com/archives/21221

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